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Radiation resistance of single and multilayer coatings against synchrotron radiation

Publikation: Beitrag in Buch/Bericht/Sammelwerk/KonferenzbandAufsatz in KonferenzbandForschungPeer-Review

Autorschaft

  • Stefan Günster
  • Holger Blaschke
  • Detlev Ristau
  • Miltcho Boyanov Danailov

Externe Organisationen

  • Laser Zentrum Hannover e.V. (LZH)
  • Sincrotrone Trieste
  • Fraunhofer-Institut für Angewandte Optik und Feinmechanik IOF
  • Ente Per Le Nuove Tecnologie L'energia e l'ambiente

Details

OriginalspracheEnglisch
Titel des SammelwerksAdvances in Optical Thin Films
Untertitel30 September - 3 October 2003, St. Etienne, France
ErscheinungsortBellingham
Herausgeber (Verlag)SPIE
Seiten146-157
Seitenumfang12
ISBN (Print)0-8194-5134-7
PublikationsstatusVeröffentlicht - 25 Feb. 2004
Extern publiziertJa
VeranstaltungAdvances in Optical Thin Films - St. Etienne, Frankreich
Dauer: 30 Sept. 20033 Okt. 2003

Publikationsreihe

NameProceedings of SPIE - The International Society for Optical Engineering
Herausgeber (Verlag)SPIE
Band5250
ISSN (Print)0277-786X

Abstract

Optical coatings for the use in free electron laser systems have to withstand high power laser radiation and the intense energetic background radiation of the synchrotron radiation source. In general, the bombardment with high energetic photons leads to irreversible changes and a discoloration of the specimen. For the development of appropriate optical coatings, the degradation mechanisms of available optical materials have to be characterized. In this contribution the degradation mechanisms of single layer coatings (fluoride and oxide materials) and multilayer systems will be presented. Fluoride and oxide single layers were produced by thermal evaporation and high energetic ion beam sputter deposition. The same methods were employed for the deposition of multilayer systems. High reflecting coatings for the wavelength region around 180nm were chosen for the irradiation tests. All samples were characterized after production by spectrophotometry covering the VUV, VIS, and MIR spectral range. Mechanical coating stress was evaluated with interferometric methods. Synchrotron irradiation tests were performed at ELETTRA, using a standardized irradiation cycle for all tests. Ambient pressure and possible contamination in the vacuum environment were monitored by mass spectrometry. For comparison, the optical coatings were investigated again in the VUV, VIS, and MIR spectral range after irradiation. On selected samples XRD measurements were performed. The observed degradation mechanisms comprise severe damages like coating and substrate surface ablation. Color centre formation in the VIS spectral range and an increase of VUV absorption were found as a major origin for a severe degradation of VUV transmittance On the basis of the performed investigations, a selection of coating materials and coating systems is possible in respect to the damage effects caused by synchrotron radiation.

ASJC Scopus Sachgebiete

Zitieren

Radiation resistance of single and multilayer coatings against synchrotron radiation. / Günster, Stefan; Blaschke, Holger; Ristau, Detlev et al.
Advances in Optical Thin Films: 30 September - 3 October 2003, St. Etienne, France. Bellingham: SPIE, 2004. S. 146-157 (Proceedings of SPIE - The International Society for Optical Engineering; Band 5250).

Publikation: Beitrag in Buch/Bericht/Sammelwerk/KonferenzbandAufsatz in KonferenzbandForschungPeer-Review

Günster, S, Blaschke, H, Ristau, D, Danailov, MB, Trovó, M, Gatto, A, Kaiser, N, Sarto, F, Flori, D & Menchini, F 2004, Radiation resistance of single and multilayer coatings against synchrotron radiation. in Advances in Optical Thin Films: 30 September - 3 October 2003, St. Etienne, France. Proceedings of SPIE - The International Society for Optical Engineering, Bd. 5250, SPIE, Bellingham, S. 146-157, Advances in Optical Thin Films, St. Etienne, Frankreich, 30 Sept. 2003. https://doi.org/10.1117/12.514801
Günster, S., Blaschke, H., Ristau, D., Danailov, M. B., Trovó, M., Gatto, A., Kaiser, N., Sarto, F., Flori, D., & Menchini, F. (2004). Radiation resistance of single and multilayer coatings against synchrotron radiation. In Advances in Optical Thin Films: 30 September - 3 October 2003, St. Etienne, France (S. 146-157). (Proceedings of SPIE - The International Society for Optical Engineering; Band 5250). SPIE. https://doi.org/10.1117/12.514801
Günster S, Blaschke H, Ristau D, Danailov MB, Trovó M, Gatto A et al. Radiation resistance of single and multilayer coatings against synchrotron radiation. in Advances in Optical Thin Films: 30 September - 3 October 2003, St. Etienne, France. Bellingham: SPIE. 2004. S. 146-157. (Proceedings of SPIE - The International Society for Optical Engineering). doi: 10.1117/12.514801
Günster, Stefan ; Blaschke, Holger ; Ristau, Detlev et al. / Radiation resistance of single and multilayer coatings against synchrotron radiation. Advances in Optical Thin Films: 30 September - 3 October 2003, St. Etienne, France. Bellingham : SPIE, 2004. S. 146-157 (Proceedings of SPIE - The International Society for Optical Engineering).
Download
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T1 - Radiation resistance of single and multilayer coatings against synchrotron radiation

AU - Günster, Stefan

AU - Blaschke, Holger

AU - Ristau, Detlev

AU - Danailov, Miltcho Boyanov

AU - Trovó, Mauro

AU - Gatto, Alexandre

AU - Kaiser, Norbert

AU - Sarto, Fransesca

AU - Flori, Daniel

AU - Menchini, F.

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N2 - Optical coatings for the use in free electron laser systems have to withstand high power laser radiation and the intense energetic background radiation of the synchrotron radiation source. In general, the bombardment with high energetic photons leads to irreversible changes and a discoloration of the specimen. For the development of appropriate optical coatings, the degradation mechanisms of available optical materials have to be characterized. In this contribution the degradation mechanisms of single layer coatings (fluoride and oxide materials) and multilayer systems will be presented. Fluoride and oxide single layers were produced by thermal evaporation and high energetic ion beam sputter deposition. The same methods were employed for the deposition of multilayer systems. High reflecting coatings for the wavelength region around 180nm were chosen for the irradiation tests. All samples were characterized after production by spectrophotometry covering the VUV, VIS, and MIR spectral range. Mechanical coating stress was evaluated with interferometric methods. Synchrotron irradiation tests were performed at ELETTRA, using a standardized irradiation cycle for all tests. Ambient pressure and possible contamination in the vacuum environment were monitored by mass spectrometry. For comparison, the optical coatings were investigated again in the VUV, VIS, and MIR spectral range after irradiation. On selected samples XRD measurements were performed. The observed degradation mechanisms comprise severe damages like coating and substrate surface ablation. Color centre formation in the VIS spectral range and an increase of VUV absorption were found as a major origin for a severe degradation of VUV transmittance On the basis of the performed investigations, a selection of coating materials and coating systems is possible in respect to the damage effects caused by synchrotron radiation.

AB - Optical coatings for the use in free electron laser systems have to withstand high power laser radiation and the intense energetic background radiation of the synchrotron radiation source. In general, the bombardment with high energetic photons leads to irreversible changes and a discoloration of the specimen. For the development of appropriate optical coatings, the degradation mechanisms of available optical materials have to be characterized. In this contribution the degradation mechanisms of single layer coatings (fluoride and oxide materials) and multilayer systems will be presented. Fluoride and oxide single layers were produced by thermal evaporation and high energetic ion beam sputter deposition. The same methods were employed for the deposition of multilayer systems. High reflecting coatings for the wavelength region around 180nm were chosen for the irradiation tests. All samples were characterized after production by spectrophotometry covering the VUV, VIS, and MIR spectral range. Mechanical coating stress was evaluated with interferometric methods. Synchrotron irradiation tests were performed at ELETTRA, using a standardized irradiation cycle for all tests. Ambient pressure and possible contamination in the vacuum environment were monitored by mass spectrometry. For comparison, the optical coatings were investigated again in the VUV, VIS, and MIR spectral range after irradiation. On selected samples XRD measurements were performed. The observed degradation mechanisms comprise severe damages like coating and substrate surface ablation. Color centre formation in the VIS spectral range and an increase of VUV absorption were found as a major origin for a severe degradation of VUV transmittance On the basis of the performed investigations, a selection of coating materials and coating systems is possible in respect to the damage effects caused by synchrotron radiation.

KW - Optics characterization

KW - Radiation resistance

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