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Influence of adding silica sand powder on the macroscopic properties and microscopic pore structures of waste-fired clay brick-based geopolymers

Research output: Contribution to journalArticleResearchpeer review

Authors

  • Cédric Mbiakop Dieuhou
  • Gaëlle Ngnie
  • Jean Jacques Kouadjo Tchekwagep
  • Barbara Rodrigue Eloundou Mbole
  • Claus Henning Rüscher

Research Organisations

External Research Organisations

  • University of Yaounde I
  • University of Jinan

Details

Original languageEnglish
Article number172
JournalArchives of Civil and Mechanical Engineering
Volume25
Issue number4
Publication statusPublished - 21 May 2025

Abstract

The task of this research is to examine the behavior of silica sand powder on the macroscopic properties and the microscopic pore structures of non-calcined and calcined waste-fired brick-based geopolymers. In the R3 reactivity test, calcined waste-fired bricks release 460 J/g, while non-calcined waste-fired bricks release 457 J/g. The findings highlight that the compressive strength of waste-fired clay brick-based geopolymers increases from (44.96 ± 1.17) to (54.45 ± 1.73) MPa after the addition of 30 g of silica sand powder. When 40 g of silica sand is added, it decreases from (54.45 ± 1.73) to (50.71 ± 1.69) MPa. The compressive strength rises from (53.16 ± 1.69) to (64.89 ± 1.96) MPa when 10 g of silica sand powder is added to the calcined waste-fired clay brick. It decreases from (64.89 ± 1.96) to (49.04 ± 1.32) MPa if 40 g of silica sand is added. The mercury intrusion porosimetry results demonstrate that the geopolymers contain mesopores and macropores. The range of pore size diameters of the calcined waste-fired clay brick-based reference geopolymer (5–60 nm) is smaller than that of the waste-fired clay brick-based geopolymer (5–94 nm). It was found that the addition of 30 and 10 g of silica sand powder to geopolymers made from non-calcined and calcined waste-fired clay bricks, respectively, tended to increase siloxane chains, convert macropores into inaccessible finer pores.

Keywords

    Compressive strength, Geopolymer materials, Microscopic pore structure, Silica sand, Surface fractal dimension, Waste fired clay brick

ASJC Scopus subject areas

Cite this

Influence of adding silica sand powder on the macroscopic properties and microscopic pore structures of waste-fired clay brick-based geopolymers. / Dieuhou, Cédric Mbiakop; Ngnie, Gaëlle; Tchekwagep, Jean Jacques Kouadjo et al.
In: Archives of Civil and Mechanical Engineering, Vol. 25, No. 4, 172, 21.05.2025.

Research output: Contribution to journalArticleResearchpeer review

Dieuhou, C. M., Ngnie, G., Tchekwagep, J. J. K., Mbole, B. R. E., Tchakouté, H. K., Li, Z., Rüscher, C. H., Nanseu-Njiki, C. P., & Hou, P. (2025). Influence of adding silica sand powder on the macroscopic properties and microscopic pore structures of waste-fired clay brick-based geopolymers. Archives of Civil and Mechanical Engineering, 25(4), Article 172. https://doi.org/10.1007/s43452-025-01222-6
Dieuhou CM, Ngnie G, Tchekwagep JJK, Mbole BRE, Tchakouté HK, Li Z et al. Influence of adding silica sand powder on the macroscopic properties and microscopic pore structures of waste-fired clay brick-based geopolymers. Archives of Civil and Mechanical Engineering. 2025 May 21;25(4):172. doi: 10.1007/s43452-025-01222-6
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AU - Dieuhou, Cédric Mbiakop

AU - Ngnie, Gaëlle

AU - Tchekwagep, Jean Jacques Kouadjo

AU - Mbole, Barbara Rodrigue Eloundou

AU - Tchakouté, Hervé Kouamo

AU - Li, Zihao

AU - Rüscher, Claus Henning

AU - Nanseu-Njiki, Charles Peguy

AU - Hou, Pengkun

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N2 - The task of this research is to examine the behavior of silica sand powder on the macroscopic properties and the microscopic pore structures of non-calcined and calcined waste-fired brick-based geopolymers. In the R3 reactivity test, calcined waste-fired bricks release 460 J/g, while non-calcined waste-fired bricks release 457 J/g. The findings highlight that the compressive strength of waste-fired clay brick-based geopolymers increases from (44.96 ± 1.17) to (54.45 ± 1.73) MPa after the addition of 30 g of silica sand powder. When 40 g of silica sand is added, it decreases from (54.45 ± 1.73) to (50.71 ± 1.69) MPa. The compressive strength rises from (53.16 ± 1.69) to (64.89 ± 1.96) MPa when 10 g of silica sand powder is added to the calcined waste-fired clay brick. It decreases from (64.89 ± 1.96) to (49.04 ± 1.32) MPa if 40 g of silica sand is added. The mercury intrusion porosimetry results demonstrate that the geopolymers contain mesopores and macropores. The range of pore size diameters of the calcined waste-fired clay brick-based reference geopolymer (5–60 nm) is smaller than that of the waste-fired clay brick-based geopolymer (5–94 nm). It was found that the addition of 30 and 10 g of silica sand powder to geopolymers made from non-calcined and calcined waste-fired clay bricks, respectively, tended to increase siloxane chains, convert macropores into inaccessible finer pores.

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