Details
| Original language | English |
|---|---|
| Pages (from-to) | 116-121 |
| Number of pages | 6 |
| Journal | KGK-Kautschuk und Gummi Kunststoffe |
| Volume | 57 |
| Issue number | 3 |
| Publication status | Published - Mar 2004 |
| Externally published | Yes |
Abstract
The HPLC-MS technique is a modern and effective method for achieving a comprehensive analysis of elutable components (extractables) from polymer materials. Applied correctly, it is superior to the classic HPLC-UV method and ideally complements the GC-MS method for the identification of thermally unstable, reactive and high-molecular analytes (molecular masses of about 100-4000 g/ mol). The HPLC-MS method does require fundamental and wide-ranging work to optimize the liquid chromatographical separation system and the ionization conditions of the mass selective detection for an effective use of the ion trap method. The ion trap method gives the possibility of forming MS/MS spectra with relatively high fragmentation from certain analytes. The MS/MS-technology requires the development of parameter specific libraries of spectra.
Keywords
- HPLC-MS, Identification of extractables, Ionization, MS/MS-technology
ASJC Scopus subject areas
- Engineering(all)
- Mechanical Engineering
- Materials Science(all)
- Polymers and Plastics
- Engineering(all)
- Industrial and Manufacturing Engineering
- Materials Science(all)
- Materials Chemistry
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In: KGK-Kautschuk und Gummi Kunststoffe, Vol. 57, No. 3, 03.2004, p. 116-121.
Research output: Contribution to journal › Article › Research › peer review
}
TY - JOUR
T1 - Identification of "Extractables" on Polymer Materials
T2 - Application of LC-MS-Technology
AU - Fichtner, S.
AU - Giese, U.
PY - 2004/3
Y1 - 2004/3
N2 - The HPLC-MS technique is a modern and effective method for achieving a comprehensive analysis of elutable components (extractables) from polymer materials. Applied correctly, it is superior to the classic HPLC-UV method and ideally complements the GC-MS method for the identification of thermally unstable, reactive and high-molecular analytes (molecular masses of about 100-4000 g/ mol). The HPLC-MS method does require fundamental and wide-ranging work to optimize the liquid chromatographical separation system and the ionization conditions of the mass selective detection for an effective use of the ion trap method. The ion trap method gives the possibility of forming MS/MS spectra with relatively high fragmentation from certain analytes. The MS/MS-technology requires the development of parameter specific libraries of spectra.
AB - The HPLC-MS technique is a modern and effective method for achieving a comprehensive analysis of elutable components (extractables) from polymer materials. Applied correctly, it is superior to the classic HPLC-UV method and ideally complements the GC-MS method for the identification of thermally unstable, reactive and high-molecular analytes (molecular masses of about 100-4000 g/ mol). The HPLC-MS method does require fundamental and wide-ranging work to optimize the liquid chromatographical separation system and the ionization conditions of the mass selective detection for an effective use of the ion trap method. The ion trap method gives the possibility of forming MS/MS spectra with relatively high fragmentation from certain analytes. The MS/MS-technology requires the development of parameter specific libraries of spectra.
KW - HPLC-MS
KW - Identification of extractables
KW - Ionization
KW - MS/MS-technology
UR - http://www.scopus.com/inward/record.url?scp=1642325528&partnerID=8YFLogxK
M3 - Article
AN - SCOPUS:1642325528
VL - 57
SP - 116
EP - 121
JO - KGK-Kautschuk und Gummi Kunststoffe
JF - KGK-Kautschuk und Gummi Kunststoffe
SN - 0948-3276
IS - 3
ER -