Luminescence dating of glacigenic deposits from northern Germany: A comparison of multigrain aliquots and single grains K-feldspar methods

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

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  • Leibniz-Institut für Angewandte Geophysik (LIAG)
  • Eberhard Karls Universität Tübingen
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OriginalspracheEnglisch
Aufsatznummer101711
FachzeitschriftQuaternary geochronology
Jahrgang91
Frühes Online-Datum6 Nov. 2025
PublikationsstatusVeröffentlicht - Jan. 2026

Abstract

Glacigenic sediments are challenging to date with luminescence dating technique, particularly with regard to resetting of the luminescence signal before sediment deposition. In this study, six samples from four different ice-marginal positions in northern Germany were investigated to test different luminescence dating methods that account for heterogeneous bleaching of meltwater deposits. Multigrain measurements exhibited agreement between fading corrected infrared stimulated luminescence (IR) and fading corrected post-infrared IR measured at 225 °C (pIRIR225) ages, suggesting the studied samples were likely well bleached, as these signals bleach at different rates. Single-grain measurements showed a high proportion of saturated grains (up to ∼33 %) in these samples. The single-grain results were therefore assessed using conventional single-grain analyses and the LnTn method. Accurate estimation of the overdispersion (OD) of a well-bleached grain population (σb) is essential for applying statistical age models. Because no suitable well-bleached analogue sample with comparable burial doses was available, σb was estimated by combining intrinsic OD (from dose recovery tests) and extrinsic OD in quadrature. Both De and Ln/Tn OD values exceeded the derived σb values, confirming that all studied samples are poorly bleached and that the Minimum Age Model (MAM) is required. MAM ages derived from conventional single-grain and LnTn approaches are generally consistent; however, standard MAM ages tend to be slightly younger than LnTn MAM ages, likely due to truncation of the De distribution through the exclusion of saturated grains. These finding demonstrate that (1) consistent IR50 and pIRIR225 ages cannot be considered a reliable indicator of well-bleached samples, and (2) σb and overdispersion values should be determined and interpreted carefully, especially for old samples with a large number of saturated grains. We recommend applying the LnTn method at the single-grain level when dating partially-bleached samples with grains close to saturation, to obtain more reliable luminescence ages.

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Luminescence dating of glacigenic deposits from northern Germany: A comparison of multigrain aliquots and single grains K-feldspar methods. / Rahimzadeh, Neda; von Soest, Niklas; Tsukamoto, Sumiko et al.
in: Quaternary geochronology, Jahrgang 91, 101711, 01.2026.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

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title = "Luminescence dating of glacigenic deposits from northern Germany: A comparison of multigrain aliquots and single grains K-feldspar methods",
abstract = "Glacigenic sediments are challenging to date with luminescence dating technique, particularly with regard to resetting of the luminescence signal before sediment deposition. In this study, six samples from four different ice-marginal positions in northern Germany were investigated to test different luminescence dating methods that account for heterogeneous bleaching of meltwater deposits. Multigrain measurements exhibited agreement between fading corrected infrared stimulated luminescence (IR) and fading corrected post-infrared IR measured at 225 °C (pIRIR225) ages, suggesting the studied samples were likely well bleached, as these signals bleach at different rates. Single-grain measurements showed a high proportion of saturated grains (up to ∼33 %) in these samples. The single-grain results were therefore assessed using conventional single-grain analyses and the LnTn method. Accurate estimation of the overdispersion (OD) of a well-bleached grain population (σb) is essential for applying statistical age models. Because no suitable well-bleached analogue sample with comparable burial doses was available, σb was estimated by combining intrinsic OD (from dose recovery tests) and extrinsic OD in quadrature. Both De and Ln/Tn OD values exceeded the derived σb values, confirming that all studied samples are poorly bleached and that the Minimum Age Model (MAM) is required. MAM ages derived from conventional single-grain and LnTn approaches are generally consistent; however, standard MAM ages tend to be slightly younger than LnTn MAM ages, likely due to truncation of the De distribution through the exclusion of saturated grains. These finding demonstrate that (1) consistent IR50 and pIRIR225 ages cannot be considered a reliable indicator of well-bleached samples, and (2) σb and overdispersion values should be determined and interpreted carefully, especially for old samples with a large number of saturated grains. We recommend applying the LnTn method at the single-grain level when dating partially-bleached samples with grains close to saturation, to obtain more reliable luminescence ages.",
keywords = "Glacigenic deposits, K-feldspar, Multigrain, Saturated grains, Single grain",
author = "Neda Rahimzadeh and {von Soest}, Niklas and Sumiko Tsukamoto and Jutta Winsemann",
note = "Publisher Copyright: {\textcopyright} 2025 The Authors",
year = "2026",
month = jan,
doi = "10.1016/j.quageo.2025.101711",
language = "English",
volume = "91",
journal = "Quaternary geochronology",
issn = "1871-1014",
publisher = "Elsevier BV",

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TY - JOUR

T1 - Luminescence dating of glacigenic deposits from northern Germany

T2 - A comparison of multigrain aliquots and single grains K-feldspar methods

AU - Rahimzadeh, Neda

AU - von Soest, Niklas

AU - Tsukamoto, Sumiko

AU - Winsemann, Jutta

N1 - Publisher Copyright: © 2025 The Authors

PY - 2026/1

Y1 - 2026/1

N2 - Glacigenic sediments are challenging to date with luminescence dating technique, particularly with regard to resetting of the luminescence signal before sediment deposition. In this study, six samples from four different ice-marginal positions in northern Germany were investigated to test different luminescence dating methods that account for heterogeneous bleaching of meltwater deposits. Multigrain measurements exhibited agreement between fading corrected infrared stimulated luminescence (IR) and fading corrected post-infrared IR measured at 225 °C (pIRIR225) ages, suggesting the studied samples were likely well bleached, as these signals bleach at different rates. Single-grain measurements showed a high proportion of saturated grains (up to ∼33 %) in these samples. The single-grain results were therefore assessed using conventional single-grain analyses and the LnTn method. Accurate estimation of the overdispersion (OD) of a well-bleached grain population (σb) is essential for applying statistical age models. Because no suitable well-bleached analogue sample with comparable burial doses was available, σb was estimated by combining intrinsic OD (from dose recovery tests) and extrinsic OD in quadrature. Both De and Ln/Tn OD values exceeded the derived σb values, confirming that all studied samples are poorly bleached and that the Minimum Age Model (MAM) is required. MAM ages derived from conventional single-grain and LnTn approaches are generally consistent; however, standard MAM ages tend to be slightly younger than LnTn MAM ages, likely due to truncation of the De distribution through the exclusion of saturated grains. These finding demonstrate that (1) consistent IR50 and pIRIR225 ages cannot be considered a reliable indicator of well-bleached samples, and (2) σb and overdispersion values should be determined and interpreted carefully, especially for old samples with a large number of saturated grains. We recommend applying the LnTn method at the single-grain level when dating partially-bleached samples with grains close to saturation, to obtain more reliable luminescence ages.

AB - Glacigenic sediments are challenging to date with luminescence dating technique, particularly with regard to resetting of the luminescence signal before sediment deposition. In this study, six samples from four different ice-marginal positions in northern Germany were investigated to test different luminescence dating methods that account for heterogeneous bleaching of meltwater deposits. Multigrain measurements exhibited agreement between fading corrected infrared stimulated luminescence (IR) and fading corrected post-infrared IR measured at 225 °C (pIRIR225) ages, suggesting the studied samples were likely well bleached, as these signals bleach at different rates. Single-grain measurements showed a high proportion of saturated grains (up to ∼33 %) in these samples. The single-grain results were therefore assessed using conventional single-grain analyses and the LnTn method. Accurate estimation of the overdispersion (OD) of a well-bleached grain population (σb) is essential for applying statistical age models. Because no suitable well-bleached analogue sample with comparable burial doses was available, σb was estimated by combining intrinsic OD (from dose recovery tests) and extrinsic OD in quadrature. Both De and Ln/Tn OD values exceeded the derived σb values, confirming that all studied samples are poorly bleached and that the Minimum Age Model (MAM) is required. MAM ages derived from conventional single-grain and LnTn approaches are generally consistent; however, standard MAM ages tend to be slightly younger than LnTn MAM ages, likely due to truncation of the De distribution through the exclusion of saturated grains. These finding demonstrate that (1) consistent IR50 and pIRIR225 ages cannot be considered a reliable indicator of well-bleached samples, and (2) σb and overdispersion values should be determined and interpreted carefully, especially for old samples with a large number of saturated grains. We recommend applying the LnTn method at the single-grain level when dating partially-bleached samples with grains close to saturation, to obtain more reliable luminescence ages.

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KW - K-feldspar

KW - Multigrain

KW - Saturated grains

KW - Single grain

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