Lipid Class Specific Quantitative Analysis of n-3 Polyunsaturated Fatty Acids in Food Supplements

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Autorschaft

  • Laura Kutzner
  • Annika I Ostermann
  • Thade Konrad
  • Dieter Riegel
  • Stefan Hellhake
  • Jan Philipp Schuchardt
  • Nils Helge Schebb

Externe Organisationen

  • Stiftung Tierärztliche Hochschule Hannover
  • Bergische Universität Wuppertal
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Details

OriginalspracheEnglisch
Seiten (von - bis)139-147
Seitenumfang9
FachzeitschriftJournal of Agricultural and Food Chemistry
Jahrgang65
Ausgabenummer1
PublikationsstatusVeröffentlicht - 11 Jan. 2017

Abstract

Supplementation products containing n-3 PUFA from marine sources serve a large market. Although the amount of eicosapentaenoic acid and docosahexaenoic acid in the products is provided by the manufacturer, no or little information is available on their lipid pattern. Therefore, we quantitatively analyzed the fatty acid pattern in the lipid fractions triglycerides, phospholipids, ethyl esters, and free fatty acids in supplementation products by means of solid phase extraction and gas chromatography. Twelve products from the European and U.S. markets containing fish, krill, algal, or plant oil were analyzed. Total n-3 PUFA content ranged from 68 g/100 g fat (fish oil) to 42 g/100 g fat (algal oil) to 17 g/100 g fat (krill oil). On the basis of the n-3 PUFA containing lipid class, the supplements can be separated dominantly in ethyl ester, re-esterified triglyceride, triglyceride, and phospholipid containing products. Algae-based products contained natural triglycerides, krill oils a complex mixture of phospholipids, triglycerides, and free fatty acids, and fish oil products either ethyl esters, re-esterified triglycerides, or triglycerides. Even products of the same class and source showed distinct differences in their lipid pattern. A specification of the lipid composition of n-3 PUFA products would allow distinguishing the different (qualities of) supplements.

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Lipid Class Specific Quantitative Analysis of n-3 Polyunsaturated Fatty Acids in Food Supplements. / Kutzner, Laura; Ostermann, Annika I; Konrad, Thade et al.
in: Journal of Agricultural and Food Chemistry, Jahrgang 65, Nr. 1, 11.01.2017, S. 139-147.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Kutzner L, Ostermann AI, Konrad T, Riegel D, Hellhake S, Schuchardt JP et al. Lipid Class Specific Quantitative Analysis of n-3 Polyunsaturated Fatty Acids in Food Supplements. Journal of Agricultural and Food Chemistry. 2017 Jan 11;65(1):139-147. doi: 10.1021/acs.jafc.6b03745
Kutzner, Laura ; Ostermann, Annika I ; Konrad, Thade et al. / Lipid Class Specific Quantitative Analysis of n-3 Polyunsaturated Fatty Acids in Food Supplements. in: Journal of Agricultural and Food Chemistry. 2017 ; Jahrgang 65, Nr. 1. S. 139-147.
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T1 - Lipid Class Specific Quantitative Analysis of n-3 Polyunsaturated Fatty Acids in Food Supplements

AU - Kutzner, Laura

AU - Ostermann, Annika I

AU - Konrad, Thade

AU - Riegel, Dieter

AU - Hellhake, Stefan

AU - Schuchardt, Jan Philipp

AU - Schebb, Nils Helge

N1 - Publisher Copyright: © 2016 American Chemical Society. Copyright: Copyright 2021 Elsevier B.V., All rights reserved.

PY - 2017/1/11

Y1 - 2017/1/11

N2 - Supplementation products containing n-3 PUFA from marine sources serve a large market. Although the amount of eicosapentaenoic acid and docosahexaenoic acid in the products is provided by the manufacturer, no or little information is available on their lipid pattern. Therefore, we quantitatively analyzed the fatty acid pattern in the lipid fractions triglycerides, phospholipids, ethyl esters, and free fatty acids in supplementation products by means of solid phase extraction and gas chromatography. Twelve products from the European and U.S. markets containing fish, krill, algal, or plant oil were analyzed. Total n-3 PUFA content ranged from 68 g/100 g fat (fish oil) to 42 g/100 g fat (algal oil) to 17 g/100 g fat (krill oil). On the basis of the n-3 PUFA containing lipid class, the supplements can be separated dominantly in ethyl ester, re-esterified triglyceride, triglyceride, and phospholipid containing products. Algae-based products contained natural triglycerides, krill oils a complex mixture of phospholipids, triglycerides, and free fatty acids, and fish oil products either ethyl esters, re-esterified triglycerides, or triglycerides. Even products of the same class and source showed distinct differences in their lipid pattern. A specification of the lipid composition of n-3 PUFA products would allow distinguishing the different (qualities of) supplements.

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KW - Phospholipids/analysis

KW - Plant Oils/chemistry

KW - Triglycerides/analysis

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KW - Lipid class

KW - Fish oil

KW - Supplements

KW - Algal oil

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JO - Journal of Agricultural and Food Chemistry

JF - Journal of Agricultural and Food Chemistry

SN - 0021-8561

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ER -

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