α-Ketol Rearrangement for Accessing Tetracyclic Natural Products

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Autorschaft

Organisationseinheiten

Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Seiten (von - bis)8154-8157
Seitenumfang4
FachzeitschriftOrganic letters
Jahrgang27
Ausgabenummer30
Frühes Online-Datum22 Juli 2025
PublikationsstatusVeröffentlicht - 1 Aug. 2025

Abstract

Tetracyclic natural products, which utilize the tetracycline skeleton, demonstrate a diverse array of biological activities. A critical structural feature of these compounds is the tertiary alcohol situated within a cis-decalin framework. In this study, we present a comprehensive protocol for the synthesis of tricyclic building blocks and complete carbon frameworks. This methodology facilitates the stereoselective synthesis of a specific enantiomer as well as its inversion to the corresponding opposite isomer via a ketol rearrangement.

ASJC Scopus Sachgebiete

Zitieren

α-Ketol Rearrangement for Accessing Tetracyclic Natural Products. / Sara, Alexandru; Eggert, Ulrike; Kalesse, Markus.
in: Organic letters, Jahrgang 27, Nr. 30, 01.08.2025, S. 8154-8157.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Sara A, Eggert U, Kalesse M. α-Ketol Rearrangement for Accessing Tetracyclic Natural Products. Organic letters. 2025 Aug 1;27(30):8154-8157. Epub 2025 Jul 22. doi: 10.1021/acs.orglett.5c02235
Sara, Alexandru ; Eggert, Ulrike ; Kalesse, Markus. / α-Ketol Rearrangement for Accessing Tetracyclic Natural Products. in: Organic letters. 2025 ; Jahrgang 27, Nr. 30. S. 8154-8157.
Download
@article{6ef9ac66a86849398152fb79d1a69a41,
title = "α-Ketol Rearrangement for Accessing Tetracyclic Natural Products",
abstract = "Tetracyclic natural products, which utilize the tetracycline skeleton, demonstrate a diverse array of biological activities. A critical structural feature of these compounds is the tertiary alcohol situated within a cis-decalin framework. In this study, we present a comprehensive protocol for the synthesis of tricyclic building blocks and complete carbon frameworks. This methodology facilitates the stereoselective synthesis of a specific enantiomer as well as its inversion to the corresponding opposite isomer via a ketol rearrangement.",
author = "Alexandru Sara and Ulrike Eggert and Markus Kalesse",
note = "Publisher Copyright: {\textcopyright} 2025 The Authors. Published by American Chemical Society",
year = "2025",
month = aug,
day = "1",
doi = "10.1021/acs.orglett.5c02235",
language = "English",
volume = "27",
pages = "8154--8157",
journal = "Organic letters",
issn = "1523-7060",
publisher = "American Chemical Society",
number = "30",

}

Download

TY - JOUR

T1 - α-Ketol Rearrangement for Accessing Tetracyclic Natural Products

AU - Sara, Alexandru

AU - Eggert, Ulrike

AU - Kalesse, Markus

N1 - Publisher Copyright: © 2025 The Authors. Published by American Chemical Society

PY - 2025/8/1

Y1 - 2025/8/1

N2 - Tetracyclic natural products, which utilize the tetracycline skeleton, demonstrate a diverse array of biological activities. A critical structural feature of these compounds is the tertiary alcohol situated within a cis-decalin framework. In this study, we present a comprehensive protocol for the synthesis of tricyclic building blocks and complete carbon frameworks. This methodology facilitates the stereoselective synthesis of a specific enantiomer as well as its inversion to the corresponding opposite isomer via a ketol rearrangement.

AB - Tetracyclic natural products, which utilize the tetracycline skeleton, demonstrate a diverse array of biological activities. A critical structural feature of these compounds is the tertiary alcohol situated within a cis-decalin framework. In this study, we present a comprehensive protocol for the synthesis of tricyclic building blocks and complete carbon frameworks. This methodology facilitates the stereoselective synthesis of a specific enantiomer as well as its inversion to the corresponding opposite isomer via a ketol rearrangement.

UR - http://www.scopus.com/inward/record.url?scp=105012852507&partnerID=8YFLogxK

U2 - 10.1021/acs.orglett.5c02235

DO - 10.1021/acs.orglett.5c02235

M3 - Article

C2 - 40693678

AN - SCOPUS:105012852507

VL - 27

SP - 8154

EP - 8157

JO - Organic letters

JF - Organic letters

SN - 1523-7060

IS - 30

ER -

Von denselben Autoren